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The HPLC eluate was electrospray directly into an Orbitrap Eclipse mass spectrometer (Thermo Fisher Scientific)

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Though legal manufacturing of fenethylline (under the brand names Captagon, Biocapton and Fitton) has been banned for nearly 40 years, illicit manufacturing has continued and is growing in scale, primarily in countries across southeastern Europe including Turkey, Bulgaria, Slovenia, Serbia and others, from where it was exported to the Near and Middle East