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Briefly, samples were prepared by serial dilution of the CS and EC extract with 10 mM ammonium acetate, and addition of [D 3 ]nicotine, [D 4 ]nornicotine, [D 4 ]anabasine and [D 4 ]anatabine as internal standard

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The monthly coefficients of variation were within an acceptable range (for TSH, free T4, and TPO Ab: 7%, 7%, and 10%, respectively)

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