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EMD Millipore) using a Vanquish Flex UHPLC (Thermo Fisher Scientific, Waltham, MA, USA) with buffer A (acetonitrile) and buffer B (20 mM ammonium carbonate, 0.1% ammonium hydroxide, pH 9)

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USADA has no authority over the NCAA, though college athletes who also compete on national and Olympic teams are subject to the world anti-doping protocols

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