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1 H NMR and 13 C NMR spectra were recorded at 300 and 75 MHz using a Brker AC300 instrument and at 600 MHz using a Brker AC600 instrument

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A 3mL or 5mL syringe is typically ideal for the initial reconstitution, while smaller 1mL insulin syringes are used for accurately measuring doses from the reconstituted solution