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The analytical standards in FDA guidance on testing methods are the benchmark for this kind of work

The valproic acid rat model of autism presents with gut bacterial dysbiosis similar to that in human autism

doi: 10.1016/bs.pmbts.2018.07.008

However, the average values for thyroxine in the diet containing 25% arugula were significantly higher than those in the diet variants with 0 and 50% arugula

The human evidence is limited, but the mechanistic rationale is enough that this remains an active research area